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Unique Operating Dynamics of Trunnion-Mounted Ball Valves

Unique Operating Dynamics of Trunnion-Mounted Ball Valves

For a very long time, the idea has exist...

Adopting the IIoT: Are Results Matching the Hype?

Adopting the IIoT: Are Results Matching the Hype?

Many valve, actuator and control manufac...

Where Valves Are Used: Everywhere!

Where Valves Are Used: Everywhere!

Valves can be found just about anywhere ...

Oxygen Cleaning: A Validated Process is Critical for Safety

Oxygen Cleaning: A Validated Process is Critical for Safety

From time to time, we re-publish well-re...

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Industry Headlines

Conference Board Economic Index Rose in October

Tuesday, 21 November 2017  |  Chris Guy

The Conference Board Leading Economic Index (LEI) for the U.S. increased 1.2% in October to 130.4 (2010 = 100), following a 0.1% increase in September...

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Industry Headlines

VanAire Celebrates Manufacturing with ‘Industry After Hours’

4 DAYS AGO
VanAire Celebrates Manufacturing with ‘Industry After Hours’

On Nov. 8, Delta County, MI K-12 students and parents attended Industry After Hours at VanAire to learn more about the high tech, high skilled manufacturing jobs that are available. Over 276 participants were treated to a fun, entertaining and informative event that exceeded expectations and inspired ...

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Emerson Opens Solutions Center in Singapore

7 DAYS AGO

As part of its drive to make Singapore a hub for the delivery of Industrial Internet of Things (IoT) technologies and services for customers across Asia Pacific, Emerson opened a customer-focused Solutions Center at the regional headquarters of its Automation Solutions business in Singapore. To mark...

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Nebraska Approves Keystone XL Pipeline Route

4 DAYS AGO

By a vote of 3-2, the Nebraska Public Service Commission approved an order giving TransCanada the go ahead to build the Keystone XL Pipeline utilizing the proposed Mainline Alternative Route. This is one of three proposed routes included in the application filed by TransCanada Keystone Pipeline. L.P...

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Energy Outlook Shows a World in Transformation

10 DAYS AGO

The resurgence in oil and gas production from the United States, deep declines in the cost of renewables and growing electrification are changing the face of the global energy system and upending traditional ways of meeting energy demand, according to the World Energy Outlook 2017 . A cleaner and more...

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Conference Board Economic Index Rose in October

3 DAYS AGO

The Conference Board Leading Economic Index (LEI) for the U.S. increased 1.2% in October to 130.4 (2010 = 100), following a 0.1% increase in September, and a 0.4% increase in August.

“The U.S. LEI increased sharply in October, as the impact of the hurricanes dissipated,” said Ataman Ozyildi...

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U.S. Industrial Output Up 0.9% in October

7 DAYS AGO

Industrial production rose 0.9% in October, and manufacturing increased 1.3%. The index for utilities rose 2.0%, but mining output fell 1.3%, as Hurricane Nate caused a sharp but short-lived decline in oil and gas drilling and extraction. Even so, industrial activity was boosted in October by a return...

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Testing High-Nickel Alloy Castings in Refineries

vmspr12_nickel_1

Refiners today are increasingly dealing with more corrosive feedstocks that present new demands on valves in the process. However, maintenance personnel can detect problems before they become major issues by using different testing methods.

In 2009, a Minnesota-located refinery was experiencing through-wall leakage with several Class 300 rotary valves tasked with controlling crude unit vacuum prefractionator charge heaters. Maintenance personnel removed insulation from the valves and noted coke residue on the surface of the valve bodies, which identified for them where the leaks were occurring (Figure 1).

vmspr12_nickel_fig1Figure 1. Removing insulation from around the ball valve in question revealed leakage locations.Fortunately, this particular situation did not result in a safety event or a fire. Instead, it illustrates how the refining industry’s use of increasingly corrosive feedstocks can combine with unknown casting defects to cause potential valve problems.


THE INVESTIGATION/ EVALUATION

Five valve body castings, all grade CW2M (cast alloy C), were returned from the refinery to the manufacturer for evaluation using both nondestructive and destructive tests.

The nondestructive tests performed on the returned castings included visual examination, pressure testing and liquid penetrant (LP) examination.

Visual examination did not reveal any signs of corrosion on the wetted casting surfaces of the returned valves, which included both as-cast and machined surfaces.

The pressure testing used water at 1125 psig (7.76 megapascals or MPa) followed by helium at 150 psig (1.0 MPa). LP testing was performed to the requirements of ASTM A903 Level III, which considers linear and rounded indications exceeding 3/16 inch (4.8 millimeters) to be relevant. The helium and hydrostatic water tests revealed no leaks. Apparently, the hydrocarbon or potential coking sealed the leak paths once the valves were brought down to ambient temperature and removed from service.

LP testing of the castings revealed indications on the exterior surface—a lesser number of indications were on the interior, cored surfaces. These indications were on both as-cast and machined surfaces. Most of the LP indications were shallow [<0.02 inch (0.5 millimeters)] and removed with minor grinding. However, on the neck area of some castings, grinding did not remove the indications. The defect progressed through the wall of the casting and could represent a leak path. (Note that all of the returned valves had through-wall leaks in the neck area.)

Destructive testing, including metallographic examination, scanning electron microscopy (SEM) and energy dispersive spectrographic analyses, was performed on several of the returned castings.

vmspr12_nickel_fig2Figure 2. Opened defect showing three zones of fracture. Original magnification 11x. For example, corrosion testing was done on one valve body casting to compare results to maximum acceptance values previously set for this material grade. The test environment was boiling ferric sulfate-sulfuric acid per ASTM G28 Practice A. Although this standard is intended for wrought product forms, the practice A test method is also useful for castings. The corrosion rate was 140 milli-inches per year or mpy (3.5 millimeters/year or mm/y) compared to the manufacturer’s acceptance criteria of 360 mpy (9.1 mm/y) maximum. The grain boundaries were visible, which is typical for this grade. Of importance to this issue is the fact that this is a very severe test that does not represent actual applications for CW2M but does detect susceptibility of weld metal and heat-affected zone to intergranular corrosion attack.

vmspr12_nickel_fig3Figure 3. Rounded dendrite fingers indicating a shrinkage defect. Original magnification 600x.Fracture surfaces from the neck area of the same valve body were examined using SEM (Figure 2). The first zone examined was an outer layer that was approximately 0.03 to 0.06 inch (0.8 to 1.5 millimeters) thick. This chill layer solidifies rapidly when the molten metal first contacts the mold surface.

The second layer or zone 2 of the fracture has a dendritic pattern. This pattern represents columnar grains that grew perpendicular from the chill layer during the balance of the solidification process. The neck was cast solid so all the grain growth was from the outer diameter to the center. The center of the neck was then bored out during machining of the casting.

Zone 3 was ductile, dimple shear. This is the fracture mode seen on any mechanical break produced in the lab.

Within the dendritic zone of some of the fractures were rounded dendrite arms (Figure 3). The rounding indicates a shrinkage defect caused by an isolated area of liquid that was frozen off from the riser system because it was not properly fed. When the liquid was consumed during solidification, the dendrite arms could not continue to grow, leaving the blunted tips. Dark areas, which were identified as oxide films formed from exposure to air during casting solidification or heat treatment, were also found on the lab fractures. This proves the fractures were present before the casting went into service.

vmspr12_nickel_fig4Figure 4. Photomicrograph showing the leak path and the continuation of the grain boundary. Original magnification 500x.Inclusions and porosity also were visible. The inclusions were mold sand, slag and oxides. The grains were very large compared to wrought product forms—about 1/4 to over 1/2 inch (6 to 13 millimeters). The grain boundaries were the intersection of the dendrites formed during solidification. One leak path was cross-sectioned (the photomicrograph in Figure 4 shows the continuation along a grain boundary).

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